Effect of hydrofluoric acid concentration and etching time on the surface roughness of CAD/CAM ceramics
نویسندگان
1
2 دانشگاه علوم پزشکی مشهد
3 دانشگاه علوم پزشکی کرمان
4 دانشگاه آزاد اسلامی
doi
10.22088/cjdr.8.2.8چکیده
Introduction: Dental ceramics are considered as materials that can restore the appearance of natural teeth. Etching the inner surface of a ceramic restoration with hydrofluoric acid (HF) followed by using a silane coupling agent is a well-known and recommended method to increase the bond strength. The aim of etching on ceramic structure is to enhance the surface roughness (Ra) and energy and to cleanse the bonding area. The aim of this study was to evaluate the effect of different HF concentrations and etching times on the Ra of IPS e.max CAD TM and Vita mark II TM . Materials & Methods: Two HF concentrations (5% and 10%) and three etching times (20, 60 and 120 seconds) were evaluated. Etched patterns were observed by scanning electron microscopy (SEM) and Ra was measured using atomic force microscopy (AFM). Surface element analysis was performed using energy dispersive X-ray spectroscopy (EDAX). Data were analyzed on SPSS 20 using ANOVA and T-test. Results: The Ra had no significant difference among various Vita mark II TM specimens (P=0.973). Among IPS e.max TM specimens etched with 5% HF, the AFM results showed that 20-s etching time had the lowest Ra and among those etched with 10% HF and 120-s etching time had the most Ra. In IPS e.max TM specimens etched with acid for 20 s, a significant difference was observed in Ra of 5% and 10% acid concentrations (5% HF lower than 10% HF) (p=0.012). Conclusion: Among IPS e.max TM specimens etched with 5% and 10% HF, increasing the etching time lead to higher Ra. For both IPS e.max TM and Vita mark II TM , 20-s etching with 5% HF provides acceptable Ra for the bond.