Synthesis and Study of the Properties of Some Metal oxide Using Co-Precipitation Method
نویسندگان
1 Department of Physics, College of Education, University of Al-Qadisiyah, Qadisiyah, Iraq
2 Department of Physics, College of Education, University of Al-Qadisiyah, Qadisiyah, Iraq
doi
10.22052/JNS.2026.01.037چکیده
In the present work, Cadimum oxide (CdxO), Manganese oxide (MnxO) and Manganese cadmium oxide (MnxCd1-xO) nanopowders (where x = 0, 0.5, and 1) were synthesized by a simple chemical co-precipitation method followed with calcination. Physical properties that reported through XRD analysis, FTIR analysis, surface morphology, and Energy dipersive X-ray spectroscopy (EDS). XRD spectra predicted the average size of synthesized CdxO nanoparticles is decreased with calcination at 700Ċ for 3 hrs while it was increased for MnxO and MnxCd1-xO The lattice constant was decreased with increasing of the crystallite size except with CdxO. The FTIR spectral analysis present reduction in the water-related peaks after calcination indicated successful removal of residual hydroxides and moisture hat help in control particle growth and lead to increase agglomeration. This result shown in FESEM micrographs revealed that the calcination process lead to increase agglomeration. The elemental composition of the nanoparticles was determined by EDS analysis.
