A rapid microwave route for the synthesis of ZnS nanoparticles
نویسندگان
1 Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P. O. Box. 87317–51167, I. R. Iran
2 Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P. O. Box. 87317–51167, I. R. Iran
3 Young Researchers Club, Arak Branch, Islamic Azad University, Arak, Iran
doi
10.7508/jns.2011.03.007چکیده
ZnS nanoparticles were synthesized via a simple surfactant free microwave route. In this synthesis, thioacetamide was used as sulfur source. The effects of different parameters such as type of zinc precursor, time and power of irradiation on the morphology and particle size of the products have been investigated. The nanostructures were characterized by means of X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) and photoluminescence (PL) spectroscopy.