Molybdenum Disulfide/Graphene Oxide Nanohybrid as an Electrocatalyst for Sensitive Detection of Carbamazepine in Human Body Fluid Samples
نویسندگان
1 Department of Chemistry, Payame Noor University, PO Box 19395-4697, Tehran, Iran
2 Department of Chemistry, Payame Noor University, PO Box 19395-4697, Tehran, Iran
3 Department of Chemistry, Payame Noor University, PO Box 19395-4697, Tehran, Iran
4 Department of Chemistry, Payame Noor University, PO Box 19395-4697, Tehran, Iran
doi
10.30473/ijac.2021.59425.1195چکیده
Molybdenum disulfide as a transition metal dichalcogenide was prepared by a hydrothermal method and hybridized with graphene oxide (MoS2/GO). The as-prepared materials were investigated by Fourier transform infra-red spectroscopy (FT-IR), X-ray diffraction (XRD), energy dispersive X-ray elemental analysis (EDX) techniques as well transmission electron microscopy (TEM) image. The nanomaterial with its electrocatalytic properties was applied as an electro-nanocatalyst for loading on a glassy carbon electrode (MoS2/GO-GCE) for detection of carbamazepine as an anti-epileptic in real body samples. The simple and low-cost developed electrochemical sensor detected carbamazepine with a vast linear concentration range(30-350nM), very low detection limit about 6.0nM and significant sensitivity equal to 0.134µA/nM.
